Production of Ξ − and Ξ − has been observed for the first time in heavy ion interactions by the WA85 Experiment. Multistrange baryon and antibaryon production is expected to be a useful probe in the search for quark-gluon plasma formation. We describe the procedure used to select these cascade candidates and show that Ξ − and Ξ − decays can be identified. The ratio of Ξ Ξ production, corrected for geometrical acceptances and reconstruction efficiencies, is 0.39 ± 0.07 for sulphur-tungsten interactions in the central rapidity interval 2.3< Y lab <3.0 and p T >1.1 GeV/ c .
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